Separating apparatus.



'H. G. PARKER. SEPARATING APPARATUS.

APPLICATION FILED JAN,9,1908.

Patented Sept. 21, 1909.

l jmWegaW/Ka HARRY G. mimmo or LIBERY; Mismo-Rr SrirfiimriimArriiiii'ris.

(fifty-in the County of Slay and SCatefo Mis; of the stziml yoke mii zi'portion of lche Myinvenio relfat'e's to" a separatfixigappshaft'a'ii'dddmpt ci for revolution ratus, and more particularly to anapparatus 0 eri' Spfice ii ei l'he yoke ai' ii' i o'c' that cla-Ss forAuse iii chemical analysis W 'el.' glouifni'ed'm a box Soli base i 15wherein the' Sepfr'ation' of a preoipitize is ltezii'lly projeofiugshiff "I, ligiving e, ,gear

i311v the separation of :i precipitate iii quarl- #he gari-oiisliufiand' n crank 9 oo iis oni ria'tive chemical analysis it has Ordinarilyenel Wiiereby the parte are' operated. L been the custom to pass theliquid containing' topz oi1v shaft 3 iw idly mouned i fue i 1M theprecipitate through a filer of paper, asfroirz opposite' de 'of Whi'oliare 'eil bestos, orother like material, which filter is the' n'rihs'1.1.7 ne ng'iili'y Secured to the, o'ui'er afterward' either ireighedwith the precipieii'rls o f sh'id arrhsii're the Semicii'jeuizrroraciotate, :mdsllowance made therefora or the lei's'a'l2; tl'ieiiomiki' paris chrieceffi thorefilter is borne@ before the We'iglfiaistaken'. ,iitlibeing (iupiica'es of en ii other; for In either oase theprecipicfre must' be in mwhich reason but on# will hereafter be rediedbefore ille Wei ht is taken,v Which to? ieii to the iorlf; with the,under- `@ether with the inoicV ent exposure lio the air, Staiifl'iiigihaft Siiiidesoripiion refers equily presents an opportunity 'for iossin trims? 'to both, Projeeying ihwarniiy from @he eh'fi fi ieri-ing, andoxidation, or from other ea'uses. of the brieliec i2 re he yi'"i'`5.,1i} oii" which l-t is ille object of' my' invention to proisirminioneii ir rin'g und projecting; vi'f'l'e alu zipparm'us wherein'the solili'on may tlu'ogii sairl, rimjiss'zi ji L51 having a Geiler beheated :md precipitation ziceoiiiplished 1G adapted fo seni :if iet amisupport the ilhouf removal from theoriginal container, jl 'fl'm lig i4:l .fomhly fiiog Wihiri iromwvhioh the liquid'nmy lie reiiio'vei'if'erjfr l5' is' a chlziiner i?, preferabiy of he preeipiiaio, :md inv whichthe precipiace less'eiier oon'ierfer shape, Whioh preerl 1i1z1"y beweighed before' being lfiariiieiE and :ibly slip-ported" on' :uiinformed iii ge ifi,

40 Withoutoxposiire to the air," zuidI Without p'reiferbiy formeiiiniegrzii yriiir L corr the use of the usual filter. lIi aloeompiishziiiii: The oontiihr 7 iSpi'oiiide'ilwi/i'h fi 25.5 irre?y this; ooieetI limite u'se of aii'or'diiiry IllllV which is nlliipted io fit SiiuglyWiiir ceutriugi'.maehinefsueh asis u'seinrlialrin or close to the niouth .of a receptcie `Q0 ing butter falo' determinatios and a"spe'oiziii Wlieir the loiterifests iieotly pri ih e hoioixji claims,reference being had to tlie" ztoco'iii d' fi. rilbhrf like sleeel for#he por pzi'nyi'u'g drawings, iii which like' reference pSe i4piiiieniin'g lakig'e through the umerl's refer to like parts throughot`the joint.V 5@ several-views, and in Whioll: operation) the liquidcoiigaip'iig the . y ceases guided by the sloping sides of the containerinto a receptaclel `Where it is highly cornpressed by the force. Afterall the precipitate has been thrown down', the liquor may be removed bydecanting,'siphon1ng, or pour' ing as desired. Should any. particles ofthe precipitate adhere to the sides of the con-v tainer they may beloosened by a swabber inI troduced through the mouth of the container.'

If it should be desired to wash the precipi tate in soine gas, or in asolution of some gas, the gas or solution may be introduced into the.container and corked in. Then When whirled the precipitate or othercompound in the container passes through the solut-ion of the gas and isWashed by it.

In case it should be desired to heat, cook, or boil some precipitate yorcompound the Whole jar and container could be placed over the burner andthe Water introduced between the jar and coiitainei-woiild act like theWater cushion in the ordinary Water bath, and the precipitate could beheated, ete., Without being removed :from the original receptacle, `andthe container in no more danger of f breaking than fiasks, etc.,- in theordinary i baths. The Water cushion serves to equalize the pressureinside the container and recep-A tacle, to prevent leakage and to'render possible the use or" a comparatively fragile material forcontainer and receptacle. The level i of the Water cushion may beslightly higher than thelevel of the liquid in the container', so thatthe liow will be slightly inward thus Washing the joint between the container and the receptacle from any portion of the precipitatingliquid.

Having thus described my invention, What I claim as new ,therein anddesire to secure by Letters Patent is l. In a separating apparatus, acontainer having a necl, and a detachable precipitate receptacle adaptedto lit over said neck, for the purpose set forth.

9.. ln a separating apparatus, a solution container having a neck at oneend, a detachable precipitate receptacle adapted for adjustment on saidneck, means for holding said receptacle to said neck, and means forrevolving said container and receptacle l around a common center, forthe purpose set forth.

3. In a separating apparatus, a solution container having a neck, adetachable pre'- cipitate receptacle adaptedto iitv over said neclr, acollar adapted` to engage a portion o'f said container and saidreceptacle, and

means for revolving said parts, for the purpose set forth.

4. ln a separating apparatus, a solution v container having a neck, adetachable precipitate .receptacle adapted to fit over said neck, and anelastic collar adapted to encentrifugal machine. The precipitate bein ggage a portion of said container and a pot*- lorced outward by thecentrifugal force 1s tion of said receptacle, for the-n purpose set'forth. l l

5. In a separating'apparatus, a suitable jar, a solution containeradapted to fit Within said jar and having a detachable precipitate exitport,and a precipitate receptacle adapti ed to seat Within saidjar andcover the exit port in said container, substantially as setl vforth.

6. ln a' separating apparatus, a suitable -jar, asolution containeradapted to lit Within Asaid jar and having a detachable precipitate exitport, .a precipitate receptacle adapted to seat on the bottom of saidjar and having a mouth adapted to cover said exit port, substantially asand for the purpose set forth.

7. In a separating apparatus, a. suitable jar, a solution containeradapted to lit within receptacle, substantially as and for the pury poseset forth.

8. `In a separating apparatus, a jar having an -internal flange, asolution container located Within said jar and seated against saidiiange, a precipitate. receptacle seated on the bottom of said jar, anda neck on said container projecting into said receptacle, substantiallyas and for the purpose set forth. I

9. Ina separating apparatus, a jar having an internal flange, a solutionreceptacle located Within said jarand seated against said iiange, adetachable precipitate receptacle seated on the bottom of said jar, aneck on said container projecting into said receptacle, and means foractuating said jar, for the purpose set forth.

10. A separating apparatus comprising a centrifugal mechanism, asuitable jar carcentrifugal mechanism,- a precipitate recep tacle, and asolution receptacle having converging sides terminating iii saidprecipitate receptacle, said receptacle being adapted for attachment toand detachment :troni saidv container'. i

i2. A separating apparatus comprising-a 'centrifugal mechanism, a lWatertight device adapted vt'or carrying ay solution container and aprecipitate receptacle, a receptacle carricd thereby, and a containercarried by said device and provided' with converging sides terminatinginsaid, receptacle, said recepdetachment from si'd container,-S'ubStansaid jar,4 and a precptterreceptabcle heatedn saidjar andconnecfg with "Sad sjoution 'containerg'both the' QQ faze beingsurroulndejby @Momma 1p said jar, said receptaclebeng adapt-d for fattachment to and detachment from sawhimper, Substantially as set forth.

, In 'tefstimony whereof I afHX my .signfatureY

